Effect of quenching temperature and filler rate on the mechanical thermal and physical properties of composites: Polypropylene/calcium carbonate

Document Type : Original research

Authors

1 Ecole Normale Supérieure de Boussaada, Boussaada 28201, Algeria

2 Laboratory of Physical Chemistry of High Polymers, Ferhat Abbas University, Setif 1-Algeria19000

3 Département de Chimie, Université Hassiba Ben Bouali de Chlef, Chlef 02180, Algeria

4 Larbi Ben M’hidi Université, Oum El Bouaghi,-Algeria 4000

5 Department of Chemistry, Laboratory of Phytochemistry and Pharmacology, University of Mohamed Seddik Benyahia, BP. 98,Ouled Aissa, Jijel, Algeria

Abstract

Polypropylene (PP) is a strong, tough, crystalline thermoplastic material with high performance. Because of its diverse thermo-physical and mechanical properties, it is utilized in a wide variety of disciplines. In this study, the impact of free quenching on the thermo-physical characteristics of PP/calcium carbonate (CaCO3) composites was examined. Three distinct heating procedures were used. First, composites were cooled from their melting phase temperature to ambient temperature. Second, composites were cooled from 130°C to a pre-determined and controlled temperature (T: 0°, 20°, 30°, 40°, 50°, 60°, 70°, 80°C). Third, composites were temperature-tested using annealing. The findings suggest that the elongation-at-break and impact strength may be improved following an initial quenching process from the melting phase to ambient temperature. On the other hand, a second quenching process at 0°C produces superior results, and a correlation between mechanical and thermal characteristics is noted; however, while these qualities are increased, others, such as flexibility, density, Vicat softening temperature (VST), and heat distortion temperature (HDT) are negatively impacted.

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Main Subjects


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  • Receive Date: 06 August 2023
  • Revise Date: 20 October 2023
  • Accept Date: 04 November 2023
  • First Publish Date: 04 November 2023